enthalpy sample 3

Measured by
Austrian Institute of Technology
Measured with NETZSCH DSC 204 F1 Phoenix
Measured according to standard
None
Comment on measurement
Crucible: Al. pan, closed. Purge gas: Nitrogen with 20 ml/min. 3 Heating & Cooling cycles between 140 and 220 °C with 10 K/min. Heat calibration performed.
Reference
Heating rate
10 K/min
Cooling rate
10 K/min
Sample mass
11.67 mg
 
Endothermic heat flow Exothermic heat flow
Value Uncertainty Value Uncertainty
Enthalpy
316.07 kJ/kg
9.68 kJ/kg
282.73 kJ/kg
2.6 kJ/kg
Integration lower limit
175.63 °C
174.6 °C
Integration upper limit
215.6 °C
147.3 °C
Onset temperature
185.93 °C
0.55 K
173.47 °C
0.33 K
Endset temperature
201.5 °C
0.53 K
159.57 °C
0.24 K
Succinic acid: Heating/cooling enthalpy measurement 3
Succinic acid: Heating/cooling enthalpy measurement 2
Succinic acid: Heating/cooling enthalpy measurement 1
Reference measurement

Succinic acid: Heating/cooling enthalpy measurement 1

Succinic acid: Heating/cooling enthalpy measurement 1

Succinic acid: Heating/cooling enthalpy measurement 2

Succinic acid: Heating/cooling enthalpy measurement 2

Succinic acid: Heating/cooling enthalpy measurement 3

Succinic acid: Heating/cooling enthalpy measurement 3