Time /min Temperature /°C Heat flow /(mW/mg) Enthalpy /(J/g) 54.48 140.01 -0.39 -293.60 54.48 140.05 -0.39 -293.61 54.47 140.08 -0.39 -293.61 54.47 140.11 -0.39 -293.61 54.47 140.15 -0.39 -293.61 54.46 140.18 -0.39 -293.61 54.46 140.21 -0.39 -293.61 54.46 140.25 -0.39 -293.61 54.45 140.28 -0.39 -293.62 54.45 140.31 -0.39 -293.62 54.45 140.35 -0.39 -293.62 54.44 140.38 -0.39 -293.62 54.44 140.41 -0.39 -293.62 54.44 140.44 -0.39 -293.62 54.43 140.48 -0.39 -293.62 54.43 140.51 -0.39 -293.63 54.43 140.54 -0.39 -293.63 54.42 140.58 -0.39 -293.63 54.42 140.61 -0.39 -293.63 54.42 140.64 -0.39 -293.63 54.41 140.68 -0.39 -293.63 54.41 140.71 -0.39 -293.63 54.41 140.74 -0.39 -293.63 54.40 140.78 -0.39 -293.64 54.40 140.81 -0.39 -293.64 54.40 140.84 -0.39 -293.64 54.39 140.88 -0.39 -293.64 54.39 140.91 -0.39 -293.64 54.39 140.94 -0.39 -293.64 54.38 140.98 -0.39 -293.64 54.38 141.01 -0.39 -293.64 54.38 141.04 -0.39 -293.64 54.37 141.08 -0.39 -293.65 54.37 141.11 -0.39 -293.65 54.37 141.14 -0.39 -293.65 54.36 141.18 -0.39 -293.65 54.36 141.21 -0.39 -293.65 54.36 141.24 -0.39 -293.65 54.35 141.28 -0.39 -293.65 54.35 141.31 -0.39 -293.65 54.35 141.34 -0.39 -293.65 54.34 141.38 -0.39 -293.65 54.34 141.41 -0.39 -293.66 54.34 141.44 -0.39 -293.66 54.33 141.48 -0.39 -293.66 54.33 141.51 -0.39 -293.66 54.33 141.54 -0.39 -293.66 54.32 141.58 -0.39 -293.66 54.32 141.61 -0.39 -293.66 54.32 141.64 -0.39 -293.66 54.31 141.68 -0.39 -293.66 54.31 141.71 -0.39 -293.66 54.31 141.74 -0.39 -293.66 54.30 141.78 -0.39 -293.66 54.30 141.81 -0.39 -293.66 54.30 141.84 -0.39 -293.66 54.29 141.88 -0.40 -293.67 54.29 141.91 -0.40 -293.67 54.29 141.94 -0.40 -293.67 54.28 141.98 -0.40 -293.67 54.28 142.01 -0.40 -293.67 54.28 142.04 -0.40 -293.67 54.27 142.08 -0.40 -293.67 54.27 142.11 -0.40 -293.67 54.27 142.14 -0.40 -293.67 54.26 142.18 -0.40 -293.67 54.26 142.21 -0.40 -293.67 54.26 142.24 -0.40 -293.67 54.25 142.28 -0.40 -293.67 54.25 142.31 -0.40 -293.67 54.25 142.34 -0.40 -293.67 54.24 142.38 -0.40 -293.67 54.24 142.41 -0.40 -293.67 54.24 142.44 -0.40 -293.67 54.23 142.48 -0.40 -293.67 54.23 142.51 -0.40 -293.67 54.23 142.54 -0.40 -293.67 54.22 142.58 -0.40 -293.67 54.22 142.61 -0.40 -293.67 54.22 142.64 -0.40 -293.67 54.21 142.68 -0.40 -293.67 54.21 142.71 -0.40 -293.67 54.21 142.74 -0.40 -293.67 54.20 142.77 -0.40 -293.67 54.20 142.81 -0.40 -293.67 54.20 142.84 -0.40 -293.67 54.19 142.87 -0.40 -293.67 54.19 142.91 -0.40 -293.67 54.19 142.94 -0.40 -293.67 54.18 142.97 -0.40 -293.67 54.18 143.01 -0.40 -293.67 54.18 143.04 -0.40 -293.67 54.17 143.07 -0.40 -293.67 54.17 143.11 -0.40 -293.67 54.17 143.14 -0.40 -293.67 54.16 143.17 -0.40 -293.67 54.16 143.21 -0.40 -293.67 54.16 143.24 -0.41 -293.66 54.15 143.27 -0.41 -293.66 54.15 143.31 -0.41 -293.66 54.15 143.34 -0.41 -293.66 54.14 143.37 -0.41 -293.66 54.14 143.41 -0.41 -293.66 54.14 143.44 -0.41 -293.66 54.13 143.47 -0.41 -293.66 54.13 143.51 -0.41 -293.66 54.13 143.54 -0.41 -293.66 54.12 143.57 -0.41 -293.66 54.12 143.61 -0.41 -293.66 54.12 143.64 -0.41 -293.65 54.11 143.67 -0.41 -293.65 54.11 143.71 -0.41 -293.65 54.11 143.74 -0.41 -293.65 54.10 143.77 -0.41 -293.65 54.10 143.81 -0.41 -293.65 54.10 143.84 -0.41 -293.65 54.09 143.87 -0.41 -293.65 54.09 143.91 -0.41 -293.65 54.09 143.94 -0.41 -293.64 54.08 143.97 -0.41 -293.64 54.08 144.01 -0.41 -293.64 54.08 144.04 -0.41 -293.64 54.07 144.07 -0.41 -293.64 54.07 144.11 -0.41 -293.64 54.07 144.14 -0.41 -293.64 54.06 144.17 -0.41 -293.63 54.06 144.21 -0.41 -293.63 54.06 144.24 -0.41 -293.63 54.05 144.27 -0.41 -293.63 54.05 144.31 -0.41 -293.63 54.05 144.34 -0.41 -293.63 54.04 144.37 -0.41 -293.62 54.04 144.41 -0.41 -293.62 54.04 144.44 -0.41 -293.62 54.03 144.47 -0.41 -293.62 54.03 144.51 -0.41 -293.62 54.03 144.54 -0.41 -293.62 54.02 144.57 -0.42 -293.61 54.02 144.61 -0.42 -293.61 54.02 144.64 -0.42 -293.61 54.01 144.67 -0.42 -293.61 54.01 144.71 -0.42 -293.61 54.01 144.74 -0.42 -293.60 54.00 144.77 -0.42 -293.60 54.00 144.81 -0.42 -293.60 54.00 144.84 -0.42 -293.60 53.99 144.87 -0.42 -293.60 53.99 144.91 -0.42 -293.59 53.99 144.94 -0.42 -293.59 53.98 144.97 -0.42 -293.59 53.98 145.00 -0.42 -293.59 53.98 145.04 -0.42 -293.58 53.97 145.07 -0.42 -293.58 53.97 145.10 -0.42 -293.58 53.97 145.14 -0.42 -293.58 53.96 145.17 -0.42 -293.57 53.96 145.20 -0.42 -293.57 53.96 145.24 -0.42 -293.57 53.95 145.27 -0.42 -293.57 53.95 145.30 -0.42 -293.56 53.95 145.34 -0.42 -293.56 53.94 145.37 -0.42 -293.56 53.94 145.40 -0.42 -293.55 53.94 145.44 -0.42 -293.55 53.93 145.47 -0.42 -293.55 53.93 145.50 -0.42 -293.55 53.93 145.54 -0.42 -293.54 53.92 145.57 -0.42 -293.54 53.92 145.60 -0.42 -293.54 53.92 145.64 -0.42 -293.53 53.91 145.67 -0.42 -293.53 53.91 145.70 -0.42 -293.53 53.91 145.74 -0.42 -293.52 53.90 145.77 -0.43 -293.52 53.90 145.81 -0.43 -293.52 53.90 145.84 -0.43 -293.51 53.89 145.87 -0.43 -293.51 53.89 145.91 -0.43 -293.51 53.89 145.94 -0.43 -293.50 53.88 145.97 -0.43 -293.50 53.88 146.01 -0.43 -293.50 53.88 146.04 -0.43 -293.49 53.87 146.07 -0.43 -293.49 53.87 146.11 -0.43 -293.49 53.87 146.14 -0.43 -293.48 53.86 146.17 -0.43 -293.48 53.86 146.21 -0.43 -293.48 53.86 146.24 -0.43 -293.47 53.85 146.27 -0.43 -293.47 53.85 146.31 -0.43 -293.46 53.85 146.34 -0.43 -293.46 53.84 146.37 -0.43 -293.46 53.84 146.41 -0.43 -293.45 53.84 146.44 -0.43 -293.45 53.83 146.47 -0.43 -293.45 53.83 146.51 -0.43 -293.44 53.83 146.54 -0.43 -293.44 53.82 146.57 -0.43 -293.43 53.82 146.61 -0.43 -293.43 53.82 146.64 -0.43 -293.42 53.81 146.67 -0.43 -293.42 53.81 146.71 -0.43 -293.42 53.81 146.74 -0.43 -293.41 53.80 146.77 -0.44 -293.41 53.80 146.81 -0.44 -293.40 53.80 146.84 -0.44 -293.40 53.79 146.87 -0.44 -293.39 53.79 146.91 -0.44 -293.39 53.79 146.94 -0.44 -293.38 53.78 146.97 -0.44 -293.38 53.78 147.01 -0.44 -293.37 53.78 147.04 -0.44 -293.37 53.77 147.07 -0.44 -293.36 53.77 147.11 -0.44 -293.36 53.77 147.14 -0.44 -293.35 53.76 147.17 -0.44 -293.35 53.76 147.21 -0.44 -293.34 53.76 147.24 -0.44 -293.34 53.75 147.27 -0.44 -293.33 53.75 147.31 -0.44 -293.33 53.75 147.34 -0.44 -293.32 53.74 147.37 -0.44 -293.31 53.74 147.41 -0.44 -293.31 53.74 147.44 -0.44 -293.30 53.73 147.47 -0.44 -293.30 53.73 147.51 -0.44 -293.29 53.73 147.54 -0.44 -293.29 53.72 147.57 -0.44 -293.28 53.72 147.61 -0.44 -293.27 53.72 147.64 -0.45 -293.27 53.71 147.67 -0.45 -293.26 53.71 147.70 -0.45 -293.26 53.71 147.74 -0.45 -293.25 53.70 147.77 -0.45 -293.24 53.70 147.80 -0.45 -293.24 53.70 147.84 -0.45 -293.23 53.69 147.87 -0.45 -293.22 53.69 147.90 -0.45 -293.22 53.69 147.94 -0.45 -293.21 53.68 147.97 -0.45 -293.20 53.68 148.00 -0.45 -293.20 53.68 148.04 -0.45 -293.19 53.67 148.07 -0.45 -293.18 53.67 148.10 -0.45 -293.18 53.67 148.14 -0.45 -293.17 53.66 148.17 -0.45 -293.16 53.66 148.20 -0.45 -293.15 53.66 148.24 -0.45 -293.15 53.65 148.27 -0.45 -293.14 53.65 148.30 -0.45 -293.13 53.65 148.34 -0.45 -293.13 53.64 148.37 -0.45 -293.12 53.64 148.40 -0.45 -293.11 53.64 148.44 -0.45 -293.10 53.63 148.47 -0.46 -293.10 53.63 148.50 -0.46 -293.09 53.63 148.54 -0.46 -293.08 53.62 148.57 -0.46 -293.07 53.62 148.60 -0.46 -293.06 53.62 148.64 -0.46 -293.06 53.61 148.67 -0.46 -293.05 53.61 148.70 -0.46 -293.04 53.61 148.74 -0.46 -293.03 53.60 148.77 -0.46 -293.02 53.60 148.80 -0.46 -293.02 53.60 148.84 -0.46 -293.01 53.59 148.87 -0.46 -293.00 53.59 148.90 -0.46 -292.99 53.59 148.93 -0.46 -292.98 53.58 148.97 -0.46 -292.97 53.58 149.00 -0.46 -292.96 53.58 149.03 -0.46 -292.95 53.57 149.07 -0.46 -292.95 53.57 149.10 -0.46 -292.94 53.57 149.13 -0.46 -292.93 53.56 149.17 -0.47 -292.92 53.56 149.20 -0.47 -292.91 53.56 149.23 -0.47 -292.90 53.55 149.27 -0.47 -292.89 53.55 149.30 -0.47 -292.88 53.55 149.33 -0.47 -292.87 53.54 149.37 -0.47 -292.86 53.54 149.40 -0.47 -292.85 53.54 149.43 -0.47 -292.84 53.53 149.47 -0.47 -292.83 53.53 149.50 -0.47 -292.82 53.53 149.53 -0.47 -292.81 53.52 149.57 -0.47 -292.80 53.52 149.60 -0.47 -292.79 53.52 149.63 -0.47 -292.78 53.51 149.67 -0.47 -292.77 53.51 149.70 -0.47 -292.76 53.51 149.73 -0.47 -292.75 53.50 149.77 -0.48 -292.74 53.50 149.80 -0.48 -292.72 53.50 149.83 -0.48 -292.71 53.49 149.87 -0.48 -292.70 53.49 149.90 -0.48 -292.69 53.49 149.93 -0.48 -292.68 53.48 149.97 -0.48 -292.67 53.48 150.00 -0.48 -292.66 53.48 150.03 -0.48 -292.65 53.47 150.07 -0.48 -292.63 53.47 150.10 -0.48 -292.62 53.47 150.13 -0.48 -292.61 53.46 150.17 -0.48 -292.60 53.46 150.20 -0.48 -292.59 53.46 150.23 -0.48 -292.57 53.45 150.27 -0.48 -292.56 53.45 150.30 -0.48 -292.55 53.45 150.33 -0.48 -292.54 53.44 150.37 -0.48 -292.52 53.44 150.40 -0.49 -292.51 53.44 150.43 -0.49 -292.50 53.43 150.47 -0.49 -292.49 53.43 150.50 -0.49 -292.47 53.43 150.53 -0.49 -292.46 53.42 150.57 -0.49 -292.45 53.42 150.60 -0.49 -292.43 53.42 150.63 -0.49 -292.42 53.41 150.66 -0.49 -292.41 53.41 150.70 -0.49 -292.39 53.41 150.73 -0.49 -292.38 53.40 150.76 -0.49 -292.37 53.40 150.80 -0.49 -292.35 53.40 150.83 -0.49 -292.34 53.39 150.86 -0.49 -292.32 53.39 150.90 -0.50 -292.31 53.39 150.93 -0.50 -292.30 53.38 150.96 -0.50 -292.28 53.38 151.00 -0.50 -292.27 53.38 151.03 -0.50 -292.25 53.37 151.06 -0.50 -292.24 53.37 151.10 -0.50 -292.22 53.37 151.13 -0.50 -292.21 53.36 151.16 -0.50 -292.19 53.36 151.20 -0.50 -292.18 53.36 151.23 -0.50 -292.16 53.35 151.26 -0.50 -292.15 53.35 151.30 -0.50 -292.13 53.35 151.33 -0.50 -292.12 53.34 151.36 -0.50 -292.10 53.34 151.40 -0.51 -292.09 53.34 151.43 -0.51 -292.07 53.33 151.46 -0.51 -292.05 53.33 151.50 -0.51 -292.04 53.33 151.53 -0.51 -292.02 53.32 151.56 -0.51 -292.01 53.32 151.60 -0.51 -291.99 53.32 151.63 -0.51 -291.97 53.31 151.66 -0.51 -291.96 53.31 151.70 -0.51 -291.94 53.31 151.73 -0.51 -291.92 53.30 151.76 -0.51 -291.90 53.30 151.80 -0.51 -291.89 53.30 151.83 -0.51 -291.87 53.29 151.86 -0.52 -291.85 53.29 151.90 -0.52 -291.83 53.29 151.93 -0.52 -291.82 53.28 151.96 -0.52 -291.80 53.28 152.00 -0.52 -291.78 53.28 152.03 -0.52 -291.76 53.27 152.06 -0.52 -291.74 53.27 152.10 -0.52 -291.72 53.27 152.13 -0.52 -291.71 53.26 152.16 -0.52 -291.69 53.26 152.20 -0.52 -291.67 53.26 152.23 -0.52 -291.65 53.25 152.26 -0.52 -291.63 53.25 152.30 -0.53 -291.61 53.25 152.33 -0.53 -291.59 53.24 152.36 -0.53 -291.57 53.24 152.40 -0.53 -291.55 53.24 152.43 -0.53 -291.53 53.23 152.46 -0.53 -291.51 53.23 152.50 -0.53 -291.49 53.23 152.53 -0.53 -291.47 53.22 152.56 -0.53 -291.45 53.22 152.60 -0.54 -291.43 53.22 152.63 -0.54 -291.40 53.21 152.66 -0.54 -291.38 53.21 152.70 -0.54 -291.36 53.21 152.73 -0.54 -291.34 53.20 152.76 -0.54 -291.32 53.20 152.80 -0.54 -291.30 53.20 152.83 -0.54 -291.27 53.19 152.86 -0.54 -291.25 53.19 152.90 -0.54 -291.23 53.19 152.93 -0.54 -291.20 53.18 152.96 -0.55 -291.18 53.18 153.00 -0.55 -291.16 53.18 153.03 -0.55 -291.13 53.17 153.06 -0.55 -291.11 53.17 153.10 -0.55 -291.09 53.17 153.13 -0.55 -291.06 53.16 153.16 -0.55 -291.04 53.16 153.20 -0.55 -291.01 53.16 153.23 -0.55 -290.99 53.15 153.26 -0.55 -290.96 53.15 153.30 -0.56 -290.94 53.15 153.33 -0.56 -290.91 53.14 153.36 -0.56 -290.89 53.14 153.40 -0.56 -290.86 53.14 153.43 -0.56 -290.84 53.13 153.46 -0.56 -290.81 53.13 153.50 -0.57 -290.78 53.13 153.53 -0.57 -290.76 53.12 153.57 -0.57 -290.73 53.12 153.60 -0.57 -290.70 53.12 153.63 -0.57 -290.67 53.11 153.67 -0.57 -290.65 53.11 153.70 -0.57 -290.62 53.11 153.73 -0.58 -290.59 53.10 153.76 -0.58 -290.56 53.10 153.80 -0.58 -290.53 53.10 153.83 -0.58 -290.50 53.09 153.86 -0.58 -290.47 53.09 153.90 -0.58 -290.44 53.09 153.93 -0.58 -290.41 53.08 153.96 -0.59 -290.38 53.08 154.00 -0.59 -290.35 53.08 154.03 -0.59 -290.32 53.07 154.06 -0.59 -290.29 53.07 154.10 -0.59 -290.26 53.07 154.13 -0.59 -290.23 53.06 154.16 -0.59 -290.19 53.06 154.20 -0.60 -290.16 53.06 154.23 -0.60 -290.13 53.05 154.26 -0.60 -290.10 53.05 154.30 -0.60 -290.06 53.05 154.33 -0.60 -290.03 53.04 154.36 -0.60 -290.00 53.04 154.40 -0.61 -289.96 53.04 154.43 -0.61 -289.93 53.03 154.46 -0.61 -289.89 53.03 154.50 -0.61 -289.86 53.03 154.53 -0.61 -289.82 53.02 154.56 -0.62 -289.78 53.02 154.60 -0.62 -289.75 53.02 154.63 -0.62 -289.71 53.01 154.66 -0.62 -289.67 53.01 154.70 -0.62 -289.64 53.01 154.73 -0.62 -289.60 53.00 154.76 -0.63 -289.56 53.00 154.80 -0.63 -289.52 53.00 154.83 -0.63 -289.48 52.99 154.86 -0.63 -289.45 52.99 154.90 -0.63 -289.41 52.99 154.93 -0.64 -289.37 52.98 154.96 -0.64 -289.33 52.98 155.00 -0.64 -289.29 52.98 155.03 -0.64 -289.24 52.97 155.06 -0.64 -289.20 52.97 155.10 -0.65 -289.16 52.97 155.13 -0.65 -289.12 52.96 155.16 -0.65 -289.08 52.96 155.20 -0.65 -289.03 52.96 155.23 -0.66 -288.99 52.95 155.26 -0.66 -288.95 52.95 155.30 -0.66 -288.90 52.95 155.33 -0.66 -288.86 52.94 155.36 -0.66 -288.81 52.94 155.40 -0.67 -288.77 52.94 155.43 -0.67 -288.72 52.93 155.46 -0.67 -288.67 52.93 155.50 -0.67 -288.63 52.93 155.53 -0.68 -288.58 52.92 155.56 -0.68 -288.53 52.92 155.60 -0.68 -288.48 52.92 155.63 -0.68 -288.43 52.91 155.66 -0.69 -288.38 52.91 155.70 -0.69 -288.33 52.91 155.73 -0.69 -288.28 52.90 155.76 -0.70 -288.23 52.90 155.80 -0.70 -288.18 52.90 155.83 -0.70 -288.13 52.89 155.86 -0.70 -288.07 52.89 155.90 -0.71 -288.02 52.89 155.93 -0.71 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