| Measured by | ZAE Bayern | |||
|---|---|---|---|---|
| Measured with | DSC Q2000 (TA Instruments) | |||
| Measured according to standard | None | |||
| Comment on measurement | No heating/cooling rate tests done. 3 samples with 2 cycles each. 0.1 wt.% nucleating agent added to influence the melting enthalpy as little as possible. Enthalpy: 5% estimated uncertainty. Different integration ranges for the crystallization enthalpy. | |||
| Reference | ||||
| Heating rate | 2 K/min | |||
| Cooling rate | 2 K/min | |||
| Sample mass | 12.375 mg | |||
| Endothermic heat flow | Exothermic heat flow | |||
| Value | Uncertainty | Value | Uncertainty | |
| Enthalpy | 198.9 kJ/kg | 9.9 kJ/kg | 192.8 kJ/kg | 9.6 kJ/kg |
| Integration lower limit | 22 °C | |||
| Integration upper limit | 37 °C | |||
| Onset temperature | 29 °C | 0.1 K | 18.5 °C | 0.5 K |
| Endset temperature | 32.2 °C | 0.1 K | ||