| Measured by | ZAE Bayern | |||
|---|---|---|---|---|
| Measured with | DSC Q2000 (TA Instruments) | |||
| Measured according to standard | None | |||
| Comment on measurement | No heating/cooling rate tests done. 3 samples with 2 cycles each. 0.1 wt.% nucleating agent added to influence the melting enthalpy as little as possible. Enthalpy: 5% estimated uncertainty. Different integration ranges for the crystallization enthalpy. | |||
| Reference | ||||
| Heating rate | 2 K/min | |||
| Cooling rate | 2 K/min | |||
| Sample mass | 12.075 mg | |||
| Endothermic heat flow | Exothermic heat flow | |||
| Value | Uncertainty | Value | Uncertainty | |
| Enthalpy | 199.2 kJ/kg | 10 kJ/kg | 193.4 kJ/kg | 9.7 kJ/kg |
| Integration lower limit | 22 °C | |||
| Integration upper limit | 37 °C | |||
| Onset temperature | 29 °C | 0.1 K | 17.9 °C | 1.1 K |
| Endset temperature | 31.7 °C | 0.8 K | ||